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dc.contributor.author박정학ko
dc.contributor.author트란녹레ko
dc.date.accessioned2015-12-17T04:51:44Z-
dc.date.available2015-12-17T04:51:44Z-
dc.date.created2015-11-13-
dc.date.issued201505-
dc.identifier.citationJOURNAL OF CHROMATOGRAPHY A, v.1396, pp.140 - 147-
dc.identifier.issn0021-9673-
dc.identifier.urihttp://hdl.handle.net/YU.REPOSITORY/32501-
dc.identifier.urihttp://dx.doi.org/10.1016/j.chroma.2015.03.085-
dc.description.abstractA weak anion-exchanger chiral selector, quinine-incorporated silica/zirconia hybrid monolithic (QUI-S/ZHM) capillary column was prepared by sol-gel technology. The performance of the QUI-S/ZHM column was investigated for enantioresolution of a set of acidic chiral drugs and dinitrobenzoyl (DNB)-amino acids by capillary electrochromatography in aqueous organic mobile phases composed of acetonitrile (ACN) and triethylammonium acetate (TEAA) buffer. Effects of several parameters including the ACN content, concentration and pH of the mobile phase on the chiral separation were examined. Baseline resolutions of all the compounds were obtained in the mobile phase consisting of 70:30 ACN/TEAA (10 mM, pH 6) under applied voltage of -10 kV at 25 degrees C within 20 min. (C) 2015 Elsevier B.V. All rights reserved.-
dc.language영어-
dc.publisherELSEVIER SCIENCE BV-
dc.subjectPERFORMANCE LIQUID-CHROMATOGRAPHY-
dc.subjectDERIVATIZED AMINO-ACIDS-
dc.subjectSTATIONARY PHASES-
dc.subjectANION-EXCHANGERS-
dc.subjectSURFACE FUNCTIONALIZATION-
dc.subjectELECTROOSMOTIC FLOW-
dc.subjectSILICA MONOLITHS-
dc.subjectCOLUMN-
dc.subjectENANTIOSEPARATION-
dc.subjectZIRCONIA-
dc.titleEnantiomer separation of acidic chiral compounds on a quinine-silica/zirconia hybrid monolith by capillary electrochromatography-
dc.typeArticle-
dc.identifier.wosid000355026900016-
dc.identifier.scopusid2-s2.0-84928766263-
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이과대학 > 화학생화학부 > Articles
문과대학 > 중국언어문화학과 > Articles
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