Sonochemical temperature controlled synthesis of pellet-, laminate- and rice grain-like morphologies of a Cu(II) porous metal-organic framework nano-structures

Title
Sonochemical temperature controlled synthesis of pellet-, laminate- and rice grain-like morphologies of a Cu(II) porous metal-organic framework nano-structures
Author(s)
주상우Azadeh Mehrani[Azadeh Mehrani]요네스피로즈살라리알리모잘리
Keywords
DESIGN
Issue Date
201407
Publisher
ELSEVIER SCIENCE BV
Citation
ULTRASONICS SONOCHEMISTRY, v.21, no.4, pp.1430 - 1434
Abstract
Nano-structures of the Cu(II) metal-organic framework, {Cu(BDT)(DMF)center dot CH3OH center dot 0.25DMF}(n) (1), which BDT2- is 1,4-benzeneditetrazolate, have been synthesized by the reaction of H2BDT with Cu(NO3)(2)center dot 6H(2)O via ultrasonic irradiation in three different temperatures, which causes different morphologies. The products were characterized by IR spectroscopy, elemental analysis, scanning electron microscopy and X-ray powder diffraction. This study demonstrates that sonochemistry is a suitable method for preparation of metal-organic framework nano-structures and temperature is an effective parameter on morphologies of Cu(II) metal-organic framework nano-structures. (C) 2014 Elsevier B.V. All rights reserved.
URI
http://hdl.handle.net/YU.REPOSITORY/31567http://dx.doi.org/10.1016/j.ultsonch.2014.01.011
ISSN
1350-4177
Appears in Collections:
공과대학 > 기계공학부 > Articles
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