Sonochemical Syntheses of a One-Dimensional Mg(II) Metal-Organic Framework: A New Precursor for Preparation of MgO One-Dimensional Nanostructure

Title
Sonochemical Syntheses of a One-Dimensional Mg(II) Metal-Organic Framework: A New Precursor for Preparation of MgO One-Dimensional Nanostructure
Author(s)
주상우Arineh Tahmasian[Arineh Tahmasian]Ali Morsali[Ali Morsali]
Keywords
LITHIUM COORDINATION POLYMER; SORPTION PROPERTIES; GAS SORPTION; BUILDING-BLOCKS; LAYER; ACID; TEMPERATURE; ADSORPTION; STABILITY; MANGANESE
Issue Date
201312
Publisher
HINDAWI PUBLISHING CORPORATION
Citation
JOURNAL OF NANOMATERIALS
Abstract
Nanostructure of a Mg-II metal-organic framework (MOF), {[Mg(HIDC)(H2O)(2)]center dot 1.5H(2)O}(n) (1) (H-3 IDC = 4,5-imidazoledicarboxylic acid), was synthesized by a sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy, and elemental analyses. The effect of concentration of starting reagents on size and morphology of nanostructured compound 1 has been studied. Calcination of the bulk powder and nanosized compound 1 at 650 degrees C under air atmosphere yields MgO nanostructures. Results show that the size and morphology of the MgO nanoparticles are dependent upon the particles size of compound 1.
URI
http://hdl.handle.net/YU.REPOSITORY/28059http://dx.doi.org/10.1155/2013/313456
ISSN
1687-4110
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공과대학 > 기계공학부 > Articles
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